Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxylamine → 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxylamine | HCID 787 | — |
| 반응물 | 1-(6-(Hydroxymethyl)pyridin-2-yl)ethanone | HCID 10329447 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime | HCID 136346367 | — |
반응 단계
To a solution of 1643 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone in 25 ml of ethanol was added 0.72 ml of a 50% aqueous hydroxylamine solution, followed by stirring overnight. The reaction solution was concentrated under reduced pressure to obtain 1806 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone oxime as an amorphous substance.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08486970B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-6ef6da3a33224778a3c3124510f154e5 |
| 출처 메모 | uspto-grants-2013_07 |