Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Aminobenzimidazole → HCID 178517650, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Aminobenzimidazole | HCID 13623 | — |
| 반응물 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 반응물 | Trimethylsilyl cyanide | HCID 82115 | — |
| 반응물 | 2-Fluoro-4-(trifluoromethyl)benzaldehyde | HCID 522929 | — |
| 생성물 | HCID 178517650 | HCID 178517650 | — |
반응 단계
The compound was synthesized starting from 5-aminobenzimidazole (0.457 g, 3.44 mmol), 2-fluoro-4-(trifluoromethyl)benzaldehyde (0.600 g, 3.13 mmol), TMSCN (0.39 mL, 3.13 mmol), PdC (10%, 0.02 g), TEA (0.455 mL, 3.26 mmol), di-(imidazol-1-yl)methanone (0.529, 3.26 mmol) as described in method 2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08486940B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-346477bc48fb46429824a6acdf4573dd |
| 출처 메모 | uspto-grants-2013_07 |