Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178517952, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 5-Aminobenzimidazole | HCID 13623 | — |
| 반응물 | Ethyl orthoformate | HCID 31214 | — |
| 반응물 | Trimethylsilyl cyanide | HCID 82115 | — |
| 반응물 | 2,3,5-Trifluorobenzaldehyde | HCID 2776950 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 생성물 | HCID 178517952 | HCID 178517952 | — |
반응 단계
The compound was synthesized starting from 5-aminobenzimidazole (0.732 g, 5.5 mmol), 2,3,5-trifluorobenzaldehyde (0.57 mL, 5 mmol), TMSCN (0.625 mL, 5 mmol), concentrated aqueous HCl (15 mL), triethyl orthoformate (30 mL, excess), NaBH4 (0.157 g, 4.14 mmol) as described in method 4.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08486940B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-e267de157ed245c98df1f1dc3ed94cdd |
| 출처 메모 | uspto-grants-2013_07 |