Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1'-Carbonyldiimidazole → HCID 178517619, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 반응물 | Trimethylsilyl cyanide | HCID 82115 | — |
| 반응물 | p-Cyclohexylbenzaldehyde | HCID 119689 | — |
| 반응물 | HCID 178507353 | HCID 178507353 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | HCID 178517619 | HCID 178517619 | — |
반응 단계
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.400 g, 3 mmol), 4-cyclohexylbenzaldehyde (0.565 g, 3 mmol), TMSCN (0.375 mL, 3 mmol), Pd/C (10%, 0.02 g), TEA 1.05 mL, 7.5 mmol), di-(imidazol-1-yl)methanone (0.730 g, 4.5 mmol) as described in method 2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08486940B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-e56637e6dea44464aadf04dd1a3636c7 |
| 출처 메모 | uspto-grants-2013_07 |