Ammonia → Butyl Acrylate

HRID 453478

반응식

HRID 453478 반응식
N.C(NN)(=O)C[CH2:4][CH2:5][CH2:6][C:7](NN)=[O:8]>O>[C:7]([O:8][CH2:7][CH2:6][CH2:5][CH3:4])(=[O:8])[CH:6]=[CH2:5]

참가 물질

4

실험 절차

In addition, as a further difference, feed stream 1 was metered in at a uniform rate over 5 minutes rather than 40 minutes, and feed stream 2 was metered in at a uniform rate over 125 minutes rather than 90 minutes. The additions of the 12.0 g of deionized water each took place following the ends of feed streams 1 and 2, and the additions of the aqueous ammonia solution took place at the same distance from the beginning of the reaction as in example 3, and, furthermore, instead of 40.9 g of a 13.2% strength by weight aqueous solution of adipic dihydrazide, 36.4 g of a 2.5% strength by weight aqueous solution of adipic dihydrazide were used.

후처리

  1. waitfeed stream 2 was metered in at a uniform rate over 125 minutes rather than 90 minutes
  2. customfrom the beginning of the reaction as in example 3

출처 및 근거

ORD 기록
ord-b2a76a84fa4f4e35a36784be012d1d33
출처 데이터셋
uspto-grants-2013_07
특허 번호
US08492472B2

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