Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,6-Dichloropyridazine → 6-chloro-N,N-dimethylpyridazin-3-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,6-Dichloropyridazine | HCID 67331 | — |
| 반응물 | Dimethylamine methanol | HCID 22497844 | — |
| 생성물 | 6-chloro-N,N-dimethylpyridazin-3-amine | HCID 252474 | 96.3% |
반응 단계
3-(N,N-Dimethylamino)-6-chloropyridazine (108f, 510 mg, 96%) was prepared in the same manner as in Example 29 as a white solid using 3,6-dichloropyridazine (107, 500 mg, 3.36 mmol) and a 2.0 M dimethylamine methanol solution (NHMe2 in MeOH, 5 mL, 10 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08497260B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-3fdef52f4ff9423e9c292be350d38a88 |
| 출처 메모 | uspto-grants-2013_07 |