Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propane sultone → 3-(3-Hexadecyl-1-imidazolio)-1-propanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propane sultone | HCID 14264 | — |
| 반응물 | 1-Hexadecyl-1H-imidazole | HCID 12415614 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 3-(3-Hexadecyl-1-imidazolio)-1-propanesulfonate | HCID 87318768 | — |
반응 단계
12.3 g of N-hexadecylimidazole was dissolved in 80 ml of acetone, and the mixture was cooled in an ice-water bath. Into the resultant, a solution in which 5.13 g of 1,3-propanesultone was dissolved in 80 ml of acetone was dripped, and after the dripping was completed, the resultant was stirred at room temperature. After the completion of the reaction, the resultant was filtered to obtain a precipitate. The precipitate was dried under reduced pressure, whereby 15.4 g of 3-(3-hexadecyl-1-imidazolio)-1-propanesulfonate (M-1) represented by the chemical formula (M-1) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541591B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-b0d4e10ac7aa4208b2090870c6d587c7 |
| 출처 메모 | uspto-grants-2013_09 |