참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 2-Thiophenecarbothioamide | HCID 737237 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Methyl thiophene-2-carbimidothioate | HCID 10487134 | 97% |
반응 단계
Methyl iodide (66 g; 0.46 mol) is added drop wise at 0° C. to a solution of thiophene-2-carbothioamide (50 g; 0.33 mol) in 500 ml of acetone. After the addition, stirring is maintained for two hours at 23° C. The precipitate formed is filtered on frit and washed twice with 100 ml of acetone before being dried under vacuum (in a bell jar). A yellow powder is obtained with a yield of 97%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07192975B2 |
|---|
| 출처 데이터셋 | uspto-grants-2007_03 |
|---|
| ORD ID | ord-8f32cc83c4a74b9aba1e5ee8bc33045c |
|---|
| 출처 메모 | uspto-grants-2007_03 |
|---|
