Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrofuran → HCID 22637025, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | Trimethyl borate | HCID 8470 | — |
| 반응물 | 4-Bromo-2-chloroanisole | HCID 3016537 | — |
| 반응물 | HCID 178418244 | HCID 178418244 | — |
| 생성물 | HCID 22637025 | HCID 22637025 | — |
반응 단계
To a THF solution of 4-bromo-2-chloroanisole was added an n-butyllithium/n-hexane solution at −78° C., followed by 30 minutes of stirring. Then, trimethyl borate was added and the whole was warmed to room temperature, followed by 30 minutes of stirring. Using the residue obtained by evaporation of the solvent instead of 3,4-dimethoxyphenylboric acid, an objective compound was obtained in a similar manner to Reference Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07196080B2 |
| 출처 데이터셋 | uspto-grants-2007_03 |
| ORD ID | ord-1115ae46fc4c4112a137d8b25c599060 |
| 출처 메모 | uspto-grants-2007_03 |