Methanol → HCID 59896206, 화합물

반응식

[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

참가 물질

반응물 2

HCID 887Methanol

HCID 99558S-(2-Aminoethyl)-L-cysteine

생성물 1

HCID 59896206HCID 59896206, 화합물

실험 절차

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

후처리

customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
concentrationthe solution was concentrated

출처 및 근거

ORD 기록: ord-4dd846f14cb74823b6db447a3bda5f9d
출처 데이터셋: uspto-grants-2007_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07196118B2

반응 노트

불러오는 중…