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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 460500생성일: 2026년 10월 25일

Phenol → 4,4,4'4'-Tetra(3-isopropyl-4-hydroxyphenyl)bicyclohexene

https://huagongshe.com/reaction/460500

반응식

참여 물질

역할이름HCID투입량
반응물PhenolHCID 996—
반응물2-IsopropylphenolHCID 6943—
반응물(1,1'-Bicyclohexyl)-4-oneHCID 41690—
용매MethanolHCID 887—
생성물4,4,4'4'-Tetra(3-isopropyl-4-hydroxyphenyl)bicyclohexeneHCID 18446146232.7%

반응 단계

The same method as specified in Reference Example 1 was used, except that 236.8 g of 0-isopropyl phenol and 23.7 g of methanol were used instead of 209.4 g of phenol and 18.9 g of methanol, and that a solution made of 39.0 g of 4,4′-bicyclohexanon and 39.0 g of 0-isopropyl phenol dissolved in 15.8 g of methanol was used instead of a solution made of 24.2 g of 4,4′-bicyclohexanon and 24.2 g of phenol dissolved in 24.2 g of methanol, to achieve reaction, neutralization, crystallization and filtering to obtain 175.9 g of 4,4,4′4′-tetra(3-isopropyl-4-hydroxyphenyl)bicyclohexene as white solid (still wet with the solution).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07196232B2
출처 데이터셋uspto-grants-2007_03
ORD IDord-615c9b1d0f7a4ec4b34e754003081310
출처 메모uspto-grants-2007_03