Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-1-methyl-1H-imidazole → 4-Methoxy-2-(1-methylimidazol-2-yl)benzo(b)furan
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-1-methyl-1H-imidazole | HCID 2773262 | — |
| 반응물 | 4-Methoxy-2-(trimethylstannyl)benzo(b)furan | HCID 22729126 | — |
| 생성물 | 4-Methoxy-2-(1-methylimidazol-2-yl)benzo(b)furan | HCID 22729146 | 53.4% |
반응 단계
By the reactions in the same manner as in Starting Material Synthesis Example 87 using 4-methoxy-2-(trimethylstannyl)benzo(b)furan (5.26 g), 2-bromo-1-methylimidazole (2.72 g) and bistriphenylphosphinepalladium dichloride (593 mg), the title compound (2.06 g) was obtained as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07196199B2 |
| 출처 데이터셋 | uspto-grants-2007_03 |
| ORD ID | ord-c0ae3ad54bfe48909422715b0dadf4a9 |
| 출처 메모 | uspto-grants-2007_03 |