Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Salicylaldehyde → alpha-(2'-Hydroxybenzylidene)-gamma-valerolactone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Salicylaldehyde | HCID 6998 | — |
| 반응물 | Gamma-Valerolactone | HCID 7921 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | alpha-(2'-Hydroxybenzylidene)-gamma-valerolactone | HCID 69497707 | 66.9% |
반응 단계
Salicylaldehyde (15.2 g) and γ-valerolactone (25 g) were dissolved in toluene (150 ml). By the reactions as in the same manner as in Example 307, the title compound (17 g) was obtained, melting point 112–114° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07196199B2 |
| 출처 데이터셋 | uspto-grants-2007_03 |
| ORD ID | ord-b7558b236a9d4731b3ff9f454b289deb |
| 출처 메모 | uspto-grants-2007_03 |