Thionyl Chloride → HCID 53698365, 화합물

반응식

[CH2:1]([C:9]1[CH:19]=[CH:18][C:12]([CH:13]=[CH:14][C:15](O)=[O:16])=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:22])=O>>[CH2:1]([C:9]1[CH:19]=[CH:18][C:12]([CH:13]=[CH:14][C:15]([Cl:22])=[O:16])=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 542659983-(4-Octylphenyl)prop-2-enoic acid

생성물 1

HCID 53698365HCID 53698365, 화합물

실험 절차

1.8 G. of p-n-octylcinnamic acid, prepared in a manner analogous to that described in Example 1, are boiled in 25 ml. of thionyl chloride for 30 minutes. The excess thionyl chloride is removed by distillation. The residue is taken up twice in absolute toluene, concentrated on a rotary evaporator and dried. There is thus obtained crude p-n-octylcinnamic acid chloride.

후처리

customThe excess thionyl chloride is removed by distillation
concentrationconcentrated on a rotary evaporator
customdried

출처 및 근거

ORD 기록: ord-019bb038b60a4c4fbb3b562d0fd56bf3
출처 데이터셋: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04061587

반응 노트

불러오는 중…