Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(3,4-dichloro-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N'-Diethylthiourea | HCID 2735009 | — |
| 반응물 | 2,3',4'-Trichloro-5'-sulfamoylacetophenone | HCID 22756445 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Ethyl-2-ethylimino-4-(3,4-dichloro-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride | HCID 21394727 | — |
반응 단계
6 g of 2,3',4'-trichloro-5'-sulfamoyl-acetophenone and 2,6 g of 1,3-diethyl-thiourea were heated for 15 minutes to 40° C in 40 ml of methanol, the 3-ethyl-2-ethylimino-4-ol-hydrochloride was precipitated with 200 ml of diisopropyl ether and crystallized from ethyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061647 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-215352d7e0b94c54832cb82d4d19c6e4 |
| 출처 메모 | uspto-grants-1977_12 |