1,4-Butanediol → Sulfamic acid, tetramethylene ester

반응식

S(O[CH2:6][CH2:7][O:8][S:9](=[O:12])(=[O:11])[NH2:10])(=O)(=O)N.[CH2:13]([OH:18])[CH2:14]CCO>>[S:9]([O:18][CH2:13][CH2:14][CH2:6][CH2:7][O:8][S:9](=[O:11])(=[O:12])[NH2:10])(=[O:11])(=[O:8])[NH2:10]

참가 물질

반응물 2

HCID 80641,4-Butanediol

HCID 148884Sulfamic acid, ethylene ester

생성물 1

HCID 148886Sulfamic acid, tetramethylene ester

실험 절차

1,4-Bis-O-sulfamyl-1,4-butanediol is prepared in the same manner as 1,2-bis-O-sulfamyl-1,2-ethanediol in Example 1 except that 1,4-butanediol (34.6 g., 0.385 mol.) is employed as the alkanediol.

출처 및 근거

ORD 기록: ord-30733bd823444943b27db5a6f25489d7
출처 데이터셋: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04061663

반응 노트

불러오는 중…