Sulfamate ion → 2,2-diphenyl-1,3-bis-O-sulfamyl-1,3-propanediol

HRID 460881

반응식

[S:1](=[O:5])(=[O:4])([O-:3])[NH2:2].[C:6]1([C:12]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)([CH2:15][OH:16])[CH2:13]O)[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([C:12]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)([CH2:15][O:16][S:1](=[O:4])(=[O:3])[NH2:2])[CH2:13][O:4][S:1](=[O:3])(=[O:5])[NH2:2])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

참가 물질

반응물 2

HCID 177700Sulfamate ion

HCID 4104452,2-Diphenylpropane-1,3-diol

생성물 1

HCID 203689762,2-diphenyl-1,3-bis-O-sulfamyl-1,3-propanediol

실험 절차

2,2-Diphenyl-1,3-bis-O-sulfamyl-1,3-propanediol is prepared in an identical manner as the sulfamate reported in Example 1 except for the use of 2,2-diphenyl-1,3-propanediol (87.7 g., 0.385 mol.) as the alkanediol.

출처 및 근거

ORD 기록: ord-7d8cbefa09b84071a2e1657d674c5784
출처 데이터셋: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04061663

연결된 노트

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