beta-Aminobeta-ethoxyacrylic acid ethyl ester → HCID 20367251, 화합물

반응식

C([O:3][C:4](=O)[CH:5]=[C:6]([NH2:10])OCC)C.[F:12][C:13]([F:25])([F:24])[O:14][C:15]1[CH:23]=[CH:22][C:18]([CH2:19][NH:20][NH2:21])=[CH:17][CH:16]=1>>[NH2:10][C:6]1[NH:21][N:20]([CH2:19][C:18]2[CH:22]=[CH:23][C:15]([O:14][C:13]([F:24])([F:25])[F:12])=[CH:16][CH:17]=2)[C:4](=[O:3])[CH:5]=1

참가 물질

반응물 2

HCID 278451beta-Aminobeta-ethoxyacrylic acid ethyl ester

HCID 203671884-Trifluoromethoxy-benzyl-hydrazine

생성물 1

HCID 20367251HCID 20367251, 화합물

실험 절차

From 17.5 g of β-amino-β-ethoxyacrylic acid ethyl ester and 20.6 g of 4-trifluoromethoxybenzylhydrazine, analogously to the procedure described in Example 1. 8.7 g of the compound identified above as colorless crystals of melting point 99°, corresponding to 32% of theory, are obtained.

후처리

customare obtained

출처 및 근거

ORD 기록: ord-fc8813197e544d508182b9223836569f
출처 데이터셋: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04061653

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