Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- → N-[(1R,2R)-2-cyclohexylcyclopentyl]piperidin-2-imine;hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- | HCID 75657 | — |
| 반응물 | o-Methylvalerolactim | HCID 138567 | — |
| 반응물 | cis-2-Cyclohexylcyclopentylamine hydrochloride | HCID 70050481 | — |
| 반응물 | rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochloride | HCID 70051154 | — |
| 생성물 | N-[(1R,2R)-2-cyclohexylcyclopentyl]piperidin-2-imine;hydrochloride | HCID 145795656 | — |
반응 단계
Following the procedure of Example 23, only substituting for cis-2-phenylcyclopentylamine hydrochloride and O-methylcaprolactim, appropriate amounts of cis-2-(cyclohexyl)cyclopentylamine hydrochloride and O-methylvalerolactim respectively the desired product is obtained, M.P. 195.5°-197° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061746 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-f7e359947188445885dbe2d74e1dd436 |
| 출처 메모 | uspto-grants-1977_12 |