Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
[6-(Hydroxymethyl)pyridin-3-yl]methanol → 5-(Hydroxymethyl)pyridine-2-carboxaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | [6-(Hydroxymethyl)pyridin-3-yl]methanol | HCID 820251 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 5-(Hydroxymethyl)pyridine-2-carboxaldehyde | HCID 13518562 | — |
반응 단계
2,5-Di(hydroxymethyl)pyridine (10 g.) in 300 ml. of hot chloroform is treated with 100 g. of manganese dioxide. After 1/2 hour of stirring, the mixture is filtered and the filtrate is evaporated to dryness to give 2-formyl-5-hydroxymethylpyridine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061759 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-710d4b0f86874e83a8868df86c633f3f |
| 출처 메모 | uspto-grants-1977_12 |