Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-Sulfamoylbenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Sulfamoylbenzoic acid | HCID 229352 | — |
| 생성물 | 3-Sulfamoylbenzoyl chloride | HCID 18801883 | — |
반응 단계
10 g of ground 3-sulfamoylbenzoic acid were reacted as prescribed in Example 70b), the thionyl chloride was distilled off and the residue was crystallized under a mixture of petroleum ether and diethyl ether (1:1). Melting point: 123° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061761 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-fd25773f3f24442092591b5bfa79d79e |
| 출처 메모 | uspto-grants-1977_12 |