Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diazomethane → 3'-Sulfamoyl-diazoacetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diazomethane | HCID 9550 | — |
| 반응물 | 3-Sulfamoylbenzoyl chloride | HCID 18801883 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3'-Sulfamoyl-diazoacetophenone | HCID 53705814 | — |
반응 단계
11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061761 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-29a7aeba45ad449fbac66113ff177cd3 |
| 출처 메모 | uspto-grants-1977_12 |