Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Magnesium peroxide (Mg(O2)) → 2-Chloro-3-methylbenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Magnesium peroxide (Mg(O2)) | HCID 61745 | — |
| 반응물 | 2-Chloro-3-methylbenzoic acid | HCID 139879 | — |
| 반응물 | Diboron | HCID 6328200 | — |
| 반응물 | (2-Chloro-3-methylphenyl)methanol | HCID 14534589 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-Chloro-3-methylbenzaldehyde | HCID 14492779 | — |
반응 단계
2-Chloro-3-methylbenzoic acid was reduced by treating with diborane in tetrahydrofuran and the resulting 2-chloro-3-methylbenzyl alcohol was oxidized with activated magnesium dioxide in methylene chloride to give 2-chloro-3-methylbenzaldehyde.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04062961 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-e128f60000ba484d87be01489aa5d34b |
| 출처 메모 | uspto-grants-1977_12 |