Water → HCID 24708775, 화합물

HRID 461519

반응식

HRID 461519 반응식
[OH:1][C:2]1[CH:12]=[CH:11][C:5]([CH2:6][CH2:7][C:8](=[O:10])[CH3:9])=[CH:4][CH:3]=1.[OH-].[K+].[CH2:15](Br)[CH:16]=[CH2:17].O>C(O)C>[CH2:17]([O:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][CH2:7][C:8](=[O:10])[CH3:9])=[CH:11][CH:12]=1)[CH:16]=[CH2:15]

참가 물질

6

반응물 4

HCID 962WaterHCID 7841Allyl bromideHCID 14797Potassium HydroxideHCID 216484-(4'-Hydroxyphenyl)-2-butanone

생성물 1

HCID 24708775HCID 24708775, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

p-Hydroxy benzylacetone (1.5 g.), KOH (6 g.) and allyl bromide (1.2 g.) were stirred in ethanol (50 ml) overnight. Water was added and the mixture extracted with ether, which was evaporated to give the compound (1.6 g.) as an oil purified by column chromatography.

후처리

  1. extractionthe mixture extracted with ether, which
  2. customwas evaporated
  3. customto give the compound (1.6 g.) as an oil
  4. custompurified by column chromatography

출처 및 근거

ORD 기록
ord-67502816a83c4a06a3fe4d307df71c29
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04062978

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