Chloride → N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

HRID 461606

반응식

HRID 461606 반응식
[CH2:1]([Cl:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH3:23])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Cl-]>>[Cl-:4].[CH2:1]([N+:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:5])[CH3:23])[CH:2]=[CH2:3]

참가 물질

4

반응물 3

HCID 312ChlorideHCID 7850Allyl chlorideHCID 16221Dimethylhexadecylamine

생성물 1

HCID 20503036N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

실험 절차

Allyl hexadecyl dimethyl ammonium chloride was prepared by reacting allyl chloride and dimethyl hexadecyl amine as set forth in Example 1. 17.8 grams of the chloride in 23.5% aqueous solution were treated with a stoichiometric excess of AgF in aqueous solution until analysis of the filtrate showed only a trace of chloride ion present. Excess silver ion was removed by the careful addition of NaCl, AgCl being removed by filtration.

후처리

  1. customExcess silver ion was removed by the careful addition of NaCl, AgCl being
  2. customremoved by filtration

출처 및 근거

ORD 기록
ord-c85224a51c4c451ebd14d9ed4e23eca9
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04064091

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