Allyl iodide → Allyl Hexadecyl Dimethyl Ammonium Iodide

HRID 461607

반응식

HRID 461607 반응식
[CH2:1]([I:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH3:23])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>C(OCC)(=O)C>[I-:4].[CH2:1]([N+:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:5])[CH3:23])[CH:2]=[CH2:3]

참가 물질

4

반응물 2

HCID 11166Allyl iodideHCID 16221Dimethylhexadecylamine

생성물 1

HCID 21391586Allyl Hexadecyl Dimethyl Ammonium Iodide

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

16.8 grams of allyl iodide were dissolved in 44.6 grams of ethyl acetate and 27.8 grams of dimethyl hexadecyl amine were added slowly with stirring at room temperature. Within 15 minutes after the addition of the amine was complete, the viscosity of the solution increased and crystallization occurred. After 24 hours the crystals were filtered, washed with ethyl acetate, and dried. The colorless crystalline product contained 88% of the theoretical amount of iodide ion.

후처리

  1. temperaturethe viscosity of the solution increased
  2. customcrystallization
  3. filtrationAfter 24 hours the crystals were filtered
  4. washwashed with ethyl acetate
  5. customdried

출처 및 근거

ORD 기록
ord-8acba59821c743c79df5910d30972d67
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04064091

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