Butyl bromide → n-Butyl diisobutylphosphinodithioate

HRID 461616노트

반응식

[CH2:1](Br)[CH2:2][CH2:3][CH3:4].[CH2:6]([P:10]([CH2:13][CH:14]([CH3:16])[CH3:15])([SH:12])=[S:11])[CH:7]([CH3:9])[CH3:8]>>[CH2:6]([P:10]([CH2:13][CH:14]([CH3:16])[CH3:15])([S:12][CH2:1][CH2:2][CH2:3][CH3:4])=[S:11])[CH:7]([CH3:9])[CH3:8]

참가 물질

반응물 2

HCID 8002Butyl bromide

HCID 83376Bis(2-methylpropyl)phosphinodithioic acid

생성물 1

HCID 21391639n-Butyl diisobutylphosphinodithioate

실험 절차

n-Butyl bromide was reacted with the ammonium salt of diisobutylphosphinodithioic acid to obtain n-butyl diisobutylphosphinodithioate, a colorless liquid, b.p. 97°-103° C at 0.05 mm. which on testing lasted 200 hours longer than the control. The total number of hours required to reach failure was 1.4 times that of the control.

출처 및 근거

ORD 기록: ord-3a1e99cf6ea44478a48789d99ce4deef
출처 데이터셋: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04064106

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