Thionyl Chloride → HCID 70637434, 화합물
반응식
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([C:8]1[C:9]([CH3:17])=[CH:10][CH:11]=[CH:12][C:13]=1[CH:14](O)[CH3:15])=[O:7].S(Cl)([Cl:20])=O>C1C=CC=CC=1>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([C:8]1[C:9]([CH3:17])=[CH:10][CH:11]=[CH:12][C:13]=1[CH:14]([Cl:20])[CH3:15])=[O:7]참가 물질
4
실험 절차
A mixture of 14.7 parts of 3-(1-hydroxyethyl)-o-tolyl 2-thienyl ketone and 126 parts of benzene is stirred while cooling on an ice-bath. Then 9.5 parts of thionyl chloride are added and the whole is stirred further over week-end at room temperature. The reaction mixture is evaporated in vacuo, yielding 3-(1-chloroethyl)-o-tolyl 2-thienyl ketone as a residue.
후처리
- temperaturewhile cooling on an ice-bath
- stirringthe whole is stirred further over week-end at room temperature
- customThe reaction mixture is evaporated in vacuo
출처 및 근거
- ORD 기록
- ord-a41ef484ee9a49528a416df6799ae2ec
- 출처 데이터셋
- uspto-grants-1977_12
- 특허 번호
- US04064132
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