Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 3-furoate → N-{2-[2-(1-Methylpiperidin-2-yl)ethyl]phenyl}furan-3-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 3-furoate | HCID 69201 | — |
| 반응물 | 2-(2-Aminophenethyl)-1-methylpiperidine | HCID 11085282 | — |
| 생성물 | N-{2-[2-(1-Methylpiperidin-2-yl)ethyl]phenyl}furan-3-carboxamide | HCID 20559948 | — |
반응 단계
Reaction of ethyl furan-3-carboxylate prepared by the method of Boyd et al, Synthesis, 545, (Oct. 1971) with 2-(2-aminophenethyl)-1-methylpiperidine according to the procedure of Example 115 provides 2'-[2-(1-methyl-2-piperidyl)ethyl]-3-furancarboxanilide, m.p. 114.5°-115.5° C (corr.), from isopropyl ether and then ethyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04064254 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-eb113b11603b47ca95fa7093ff3a8dc0 |
| 출처 메모 | uspto-grants-1977_12 |