Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Aminophenoxy)benzene → 1-(4-Phenoxyphenyl)piperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Aminophenoxy)benzene | HCID 8764 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Bis(2-bromoethyl)amine | HCID 415719 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1-(4-Phenoxyphenyl)piperazine | HCID 3017356 | — |
반응 단계
To a solution of 62.4 parts of bis-(β-bromoethyl)amine dihybromide in 160 parts of methanol there were added 37 parts of para-phenoxyaniline. The mixture was refluxed for 10 hours. 10.6 parts of Na2CO3 were then added and the reaction mixture was refluxed for a further 10 hours. After cooling, the precipitate was filtered off, washed with 80 parts of methanol and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04064245 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-2368a7cc6aa643bf82c15e20288aef90 |
| 출처 메모 | uspto-grants-1977_12 |