Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| 반응물 | Acetanilide, 2-chloro-4'-nitro- | HCID 140220 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733006 | — |
반응 단계
In a manner similar to that described above in 1a, and using 14.2 parts of N-(3-dimethylaminopropyl)formamide, 20.0 parts of 2-chloro-4'-nitroacetanilide, and 78 parts of isopropyl alcohol there was obtained 27.4 parts of N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid which melted at 195°-196° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04065500 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-402c1ace94fc4ca599dadaf99a086bcf |
| 출처 메모 | uspto-grants-1977_12 |