Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(5-nitro-1-naphthylmethyl)-N-3-formamidopropylammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| 반응물 | 1-Chloromethyl-5-nitronaphthalene | HCID 226047 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N,N-dimethyl-N-(5-nitro-1-naphthylmethyl)-N-3-formamidopropylammonium chloride | HCID 86733015 | — |
반응 단계
Proceeding in a manner similar to that described above in B-8a, 29.9 parts of N-(3-dimethylaminopropyl)formamide and 44.3 parts of 5-nitro-1-chloromethylnaphthalene were interacted in 30 parts of water to obtain N,N-dimethyl-N-(5-nitro-1-naphthylmethyl)-N-3-formamidopropylammonium chloride. The product was not isolated but was used directly in solution for reduction of the nitro group.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04065500 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-d69c34ab2e404d4d861b8dabae9686a3 |
| 출처 메모 | uspto-grants-1977_12 |