Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-Butylamine → 2-(2-t-Butylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-Butylamine | HCID 6385 | — |
| 반응물 | Cyclohexylamine | HCID 7965 | — |
| 반응물 | 2-(2-Cyclohexylamino-5-thiadiazolyl)-1-methyl-5nitroimidazole | HCID 21390861 | — |
| 생성물 | 2-(2-t-Butylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole | HCID 21390806 | — |
반응 단계
The preparation of the above compound is accomplished essentially by the procedure described for the 2-cyclohexylamino derivative (Example 38), an equivalent of t-butylamine replacing the cyclohexylamine. Recrystallization of the crude product from a mixture of ethyl acetate and acetone gives the pure compound melting at 249°-251° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04065567 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-73ab2a9a9569489d90ea3ede1479815f |
| 출처 메모 | uspto-grants-1977_12 |