Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexylamine → 2-(2-n-Octylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexylamine | HCID 7965 | — |
| 반응물 | Octylamine | HCID 8143 | — |
| 반응물 | 2-(2-Cyclohexylamino-5-thiadiazolyl)-1-methyl-5nitroimidazole | HCID 21390861 | — |
| 생성물 | 2-(2-n-Octylamino-5-thiadiazolyl)-1-methyl-5-nitroimidazole | HCID 68120260 | — |
반응 단계
The preparation of the above compound is carried out essentially as described for the 2-cyclohexylamino derivative (Example 38), an equivalent of n-octylamine replacing the cyclohexylamine. The crude product is purified by recrystallization from aqueous 2-methoxyethanol and then melts at 130°-132° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04065567 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-753b35837da44544a0a6e1d524189248 |
| 출처 메모 | uspto-grants-1977_12 |