Sodium Methoxide → 2-Cyclopropyl-4-methoxy-6-(trichloromethyl)-1,3,5-triazine

HRID 462338노트

반응식

HRID 462338 반응식
[CH:1]1([C:4]2[N:9]=[C:8](C(Cl)(Cl)Cl)[N:7]=[C:6]([C:14]([Cl:17])([Cl:16])[Cl:15])[N:5]=2)[CH2:3][CH2:2]1.[CH3:18][O-:19].[Na+]>CO>[CH:1]1([C:4]2[N:9]=[C:8]([O:19][CH3:18])[N:7]=[C:6]([C:14]([Cl:17])([Cl:16])[Cl:15])[N:5]=2)[CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 10942334Sodium MethoxideHCID 201996132-Cyclopropyl-4,6-bis-trichloromethyl-1,3,5-triazine

생성물 1

HCID 201996182-Cyclopropyl-4-methoxy-6-(trichloromethyl)-1,3,5-triazine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To a solution of 48 g of 2-cyclopropyl-4,6-bis-(trichloromethyl)-1,3,5-triazine in 200 ml of MeOH are added, with stirring, 4.9 g of sodium methylate, and the mixture is stirred for 1 hour at room temperature; it is then filtered and the filtrate is evaporated to dryness. The yield is 28.5 g of the title compound as a light-red oil, which solidifies after some time, m.p. 49°-51° C.

후처리

  1. filtrationit is then filtered
  2. customthe filtrate is evaporated to dryness

출처 및 근거

ORD 기록
ord-123c62b60c094bd3809ef41bb9934d9e
출처 데이터셋
uspto-grants-1985_05
특허 번호
US04515626

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