참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acrylamide | HCID 6579 | — |
| 반응물 | Acrylic Acid | HCID 6581 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Acrylamide-acrylic acid resin | HCID 62693 | — |
반응 단계
56 grams 50% acrylamide, 12 grams acrylic acid and 127 grams water were mixed, and warmed up to 30° C. Nitrogen was used to purge the flask. Then 0.7 gram ammonium persulfate in 3 grams of water and 0.7 gram sodium metabisulfite in 3 grams water were added, respectively. After 20 minutes, the reaction began to take place, the temperature slowly rose to 78° C. (max.) after stirring for 1.5 hour a 20% copolymer was thus produced with an acrylamide/acrylic acid ratio of 70/30. 7 grams NaOH in 30 grams water was then added to neutralize the copolymer.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04515855 |
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| 출처 데이터셋 | uspto-grants-1985_05 |
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| ORD ID | ord-afb2cfbf8f8b4735958f3371f9372578 |
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| 출처 메모 | uspto-grants-1985_05 |
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