9,10-Anthracenedicarboxaldehyde → 9,10-Anthracenedicarboxaldehyde, dihydrochloride

HRID 462508

반응식

HRID 462508 반응식
[CH:1]1[C:14]2[C:5](=[C:6]([CH:17]=[O:18])[C:7]3[C:12]([C:13]=2[CH:15]=[O:16])=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH:4]=[CH:3][CH:2]=1.[ClH:19].Cl.N(C1NCCN=1)N>C(O)CC>[ClH:19].[ClH:19].[CH:8]1[C:7]2[C:12](=[C:13]([CH:15]=[O:16])[C:14]3[C:5]([C:6]=2[CH:17]=[O:18])=[CH:4][CH:3]=[CH:2][CH:1]=3)[CH:11]=[CH:10][CH:9]=1

참가 물질

4

반응물 2

HCID 815009,10-AnthracenedicarboxaldehydeHCID 122212312-Hydrazinoimidazoline dihydrochloride

생성물 1

HCID 197628419,10-Anthracenedicarboxaldehyde, dihydrochloride

시약·촉매·용매 1

HCID 10311-Propanol용매

실험 절차

A suspension of 5.0 g of 9,10-anthracenedicarboxaldehyde and 7.8 g of 2-hydrazino-2-imidazoline dihydrochloride in 75 ml of n-propanol is refluxed for 2 hours. The mixture is cooled and the solid is collected giving bis(2-imidazolin-2-ylhydrazone) of 9,10-anthracenedicarboxaldehyde, dihydrochloride.

후처리

  1. temperatureis refluxed for 2 hours
  2. temperatureThe mixture is cooled
  3. customthe solid is collected

출처 및 근거

ORD 기록
ord-3a2581060dba434faf9facaffd8891e3
출처 데이터셋
uspto-grants-1985_05
특허 번호
US04515954

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