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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 462820생성일: 2026년 10월 25일

Chlorine → Pyridine, 2,3,4,5-tetrachloro-6-(trichloromethyl)-

https://huagongshe.com/reaction/462820

반응식

참여 물질

역할이름HCID투입량
반응물ChlorineHCID 24526—
반응물Pyridine, 3,4,5-trichloro-2-(trichloromethyl)-HCID 70990—
생성물Pyridine, 2,3,4,5-tetrachloro-6-(trichloromethyl)-HCID 7081165%

반응 단계

Summarizing Example 1, starting with fifty grams of a mixture rich in 3,4,5-trichloro-2-trichloromethyl pyridine, the analysis of which is set forth in Table One, and which contained 3% by weight ferric chloride, its chlorination with 70 grams per hour of chlorine, sparged into a 250 ml glass reactor at 200° C. for 5 hours, resulted in a product the analysis of which is set forth in Table One. As will be noted, a molar yield in excess of 65% of 3,4,5,6-tetrachloro-2-trichloromethyl pyridine based on 3,4,5-trichloro-2-trichloromethyl pyridine conversion was obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04517369
출처 데이터셋uspto-grants-1985_05
ORD IDord-15312b5ae56c4930b6453021c4f264c6
출처 메모uspto-grants-1985_05