Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorine → Pyridine, 2,3,4,5-tetrachloro-6-(trichloromethyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorine | HCID 24526 | — |
| 반응물 | Pyridine, 3,4,5-trichloro-2-(trichloromethyl)- | HCID 70990 | — |
| 생성물 | Pyridine, 2,3,4,5-tetrachloro-6-(trichloromethyl)- | HCID 70811 | 65% |
반응 단계
Summarizing Example 1, starting with fifty grams of a mixture rich in 3,4,5-trichloro-2-trichloromethyl pyridine, the analysis of which is set forth in Table One, and which contained 3% by weight ferric chloride, its chlorination with 70 grams per hour of chlorine, sparged into a 250 ml glass reactor at 200° C. for 5 hours, resulted in a product the analysis of which is set forth in Table One. As will be noted, a molar yield in excess of 65% of 3,4,5,6-tetrachloro-2-trichloromethyl pyridine based on 3,4,5-trichloro-2-trichloromethyl pyridine conversion was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04517369 |
| 출처 데이터셋 | uspto-grants-1985_05 |
| ORD ID | ord-15312b5ae56c4930b6453021c4f264c6 |
| 출처 메모 | uspto-grants-1985_05 |