Thionyl Chloride → HCID 178444542, 화합물

HRID 462875

반응식

HRID 462875 반응식
[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([OH:14])=O)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5].S(Cl)([Cl:17])=O>>[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([Cl:17])=[O:14])[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 178444557HCID 178444557, 화합물

생성물 1

HCID 178444542HCID 178444542, 화합물

실험 절차

5.58 g Of trans-4-pentylcyclohexylcarboxylic acid was heated with 20 ml of thionyl chloride under reflux conditions. After the reaction was completed, the excess of thionyl chloride was removed completely under reduced pressure and the product residue obtained was distilled under reduced pressure. Trans-4-pentylcyclohexylcarbonyl chloride having a boiling point of 103° to 105° C./0.5 mmHg was obtained.

후처리

  1. customthe excess of thionyl chloride was removed completely under reduced pressure
  2. customthe product residue obtained
  3. distillationwas distilled under reduced pressure

출처 및 근거

ORD 기록
ord-a6066b6dbaaa4fe79ddd37f85dbd565e
출처 데이터셋
uspto-grants-1985_05
특허 번호
US04518226

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