3,4-Dimethoxybenzene-1-thiol → 8-[4-(3,4-Dimethoxy-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463184노트

반응식

HRID 463184 반응식
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[C:16]2[NH:15][C:14](=[O:17])[O:13][C:12]([CH3:19])([CH3:18])[C:11]=2[CH:10]=[CH:9][CH:8]=1.[CH3:20][O:21][C:22]1[CH:23]=[C:24]([SH:30])[CH:25]=[CH:26][C:27]=1[O:28][CH3:29]>>[CH3:20][O:21][C:22]1[CH:23]=[C:24]([S:30][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[C:16]3[NH:15][C:14](=[O:17])[O:13][C:12]([CH3:19])([CH3:18])[C:11]=3[CH:10]=[CH:9][CH:8]=2)[CH:25]=[CH:26][C:27]=1[O:28][CH3:29]

참가 물질

3

반응물 2

HCID 1365393,4-Dimethoxybenzene-1-thiolHCID 202817738-(4-chlorobutoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

생성물 1

HCID 202816738-[4-(3,4-Dimethoxy-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

실험 절차

Prepared analogously to Example 1 from 8-(4-chlorobutoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dimethoxy-thiophenol.

출처 및 근거

ORD 기록
ord-0a63340315854db0b81ec0350959dc0e
출처 데이터셋
uspto-grants-1985_05
특허 번호
US04518597

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