Hydrogen Peroxide → 6-[4-(3,4-Dichloro-phenylsulfinyl)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

반응식

[Cl:1][C:2]1[CH:3]=[C:4]([S:9][CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:16]=[C:17]([CH3:28])[C:18]3[NH:23][C:22](=[O:24])[O:21][C:20]([CH3:26])([CH3:25])[C:19]=3[CH:27]=2)[CH:5]=[CH:6][C:7]=1[Cl:8].[OH:29]O>>[Cl:1][C:2]1[CH:3]=[C:4]([S:9]([CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:16]=[C:17]([CH3:28])[C:18]3[NH:23][C:22](=[O:24])[O:21][C:20]([CH3:25])([CH3:26])[C:19]=3[CH:27]=2)=[O:29])[CH:5]=[CH:6][C:7]=1[Cl:8]

참가 물질

반응물 2

HCID 784Hydrogen Peroxide

HCID 202817106-[4-(3,4-Dichloro-phenylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

생성물 1

HCID 202816996-[4-(3,4-Dichloro-phenylsulfinyl)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

실험 절차

Prepared analogously to Example 2 from 6-[4-(3,4-dichloro-phenylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

출처 및 근거

ORD 기록: ord-ca7269a894d14ed4ba7c66ded764ede4
출처 데이터셋: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04518597

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