Hydrogen Peroxide → 6-[4-(4-Chloro-phenylsulfinyl)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

반응식

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:15]=[C:16]([CH3:27])[C:17]3[NH:22][C:21](=[O:23])[O:20][C:19]([CH3:25])([CH3:24])[C:18]=3[CH:26]=2)=[CH:4][CH:3]=1.[OH:28]O>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:15]=[C:16]([CH3:27])[C:17]3[NH:22][C:21](=[O:23])[O:20][C:19]([CH3:24])([CH3:25])[C:18]=3[CH:26]=2)=[O:28])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 784Hydrogen Peroxide

HCID 202818596-[4-(4-Chloro-phenylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

생성물 1

HCID 202816896-[4-(4-Chloro-phenylsulfinyl)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

실험 절차

Prepared analogously to Example 2 from 6-[4-(4-chloro-phenylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

출처 및 근거

ORD 기록: ord-64999600482e4ab88ee0e1424666f38b
출처 데이터셋: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04518597

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