Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → 1-Chloro-4-(3-phenylpropyl)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 4'-Chloro-3-phenylpropiophenone | HCID 247344 | — |
| 용매 | Diethylene Glycol | HCID 8117 | — |
| 생성물 | 1-Chloro-4-(3-phenylpropyl)benzene | HCID 13300857 | — |
반응 단계
p-chlorophenyl phenylethyl ketone (25 g) was refluxed with hydrazine hydrate (13 g) and potassium hydroxide (18 g) in Digol (diethylene glycol) for one hour. The mixture was then distilled until the solution temperature in the still reached 175°. The mixture was then refluxed for 3 hours, cooled, poured into water and extracted with petroleum ether (Bpt 40°-60°). Evaporation of the extracts gave 1-(4-chlorophenyl)-3-phenylpropane Bbt. 110°/10-3 mm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04520007 |
| 출처 데이터셋 | uspto-grants-1985_05 |
| ORD ID | ord-3ea19a854acc474080cbdd3124680918 |
| 출처 메모 | uspto-grants-1985_05 |