Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Dinitrobenzene → HCID 13292704, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Dinitrobenzene | HCID 10707 | — |
| 반응물 | Diethyl methylphosphonite | HCID 85063 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 13292704 | HCID 13292704 | — |
반응 단계
A mixture of 1,2-dinitrobenzene (2.48 mmol), diethyl methylphosphonite (3.72 mmol) and acetonitrile (3 ml) is stirred at RT overnight. The reaction is concentrated to dryness, and the residue is purified by preparative thin layer chromatography (TLC) to yield ethyl P-methyl-2-nitrophenyl-phosphinate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04520197 |
| 출처 데이터셋 | uspto-grants-1985_05 |
| ORD ID | ord-c34ce62fdba4431e8122437a12d3da68 |
| 출처 메모 | uspto-grants-1985_05 |