1,2-Dinitrobenzene → HCID 13292704, 화합물

HRID 463551

반응식

HRID 463551 반응식
[N+]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N+:10]([O-:12])=[O:11])([O-])=O.[CH3:13][P:14]([O:18]CC)[O:15][CH2:16][CH3:17]>C(#N)C>[CH3:13][P:14]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N+:10]([O-:12])=[O:11])(=[O:18])[O:15][CH2:16][CH3:17]

참가 물질

4

반응물 2

HCID 107071,2-DinitrobenzeneHCID 85063Diethyl methylphosphonite

생성물 1

HCID 13292704HCID 13292704, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

A mixture of 1,2-dinitrobenzene (2.48 mmol), diethyl methylphosphonite (3.72 mmol) and acetonitrile (3 ml) is stirred at RT overnight. The reaction is concentrated to dryness, and the residue is purified by preparative thin layer chromatography (TLC) to yield ethyl P-methyl-2-nitrophenyl-phosphinate.

후처리

  1. concentrationThe reaction is concentrated to dryness
  2. customthe residue is purified by preparative thin layer chromatography (TLC)

출처 및 근거

ORD 기록
ord-c34ce62fdba4431e8122437a12d3da68
출처 데이터셋
uspto-grants-1985_05
특허 번호
US04520197

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