Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-1,2-dinitrobenzene → ethyl P-methyl-2-nitro-5-chlorophenylphosphinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-1,2-dinitrobenzene | HCID 33097 | — |
| 반응물 | Diethyl methylphosphonite | HCID 85063 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | ethyl P-methyl-2-nitro-5-chlorophenylphosphinate | HCID 53860251 | — |
반응 단계
A mixture of 4-chloro-1,2-dinitrobenzene (3.31 mmol) and diethyl methylphosphonite (5.30 mmol) in 3 ml of acetonitrile is stirred at RT overnight. The mixture is then concentrated and the residue is purified by preparative TLC to yield ethyl P-methyl-2-nitro-5-chlorophenylphosphinate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04520197 |
| 출처 데이터셋 | uspto-grants-1985_05 |
| ORD ID | ord-d946924498814018b352a39df226c1bf |
| 출처 메모 | uspto-grants-1985_05 |