Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Dichlorophenol → N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Dichlorophenol | HCID 8449 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | n-(2,3-Dichloro-6-nitrophenyl)acetamide | HCID 291466 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264352 | — |
반응 단계
A mixture of N-methylcarbonyl 2,3-dichloro-6-nitroaniline (0.90 g, 3.6 mmol), 2,4-dichloro-phenol (0.59 g, 3.6 mmol) and potassium carbonate (1.0 g, 7.2 mmol), in 20 ml of DMSO, is stirred at 90° for 3 hours. The reaction is then cooled and poured onto about 60 g of ice. A yellow solid is collected by filtration to give N-methylcarbonyl 2-chloro-3-(2,4-dichloro-phenoxy)-6-nitroaniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04544400 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-58f846855fe64b879956baeae0e90178 |
| 출처 메모 | uspto-grants-1985_10 |