Methylamine → HCID 19836622, 화합물
반응식
[CH3:1][C:2]1([CH3:13])[CH2:4][N:3]1[P:5](Br)([N:7]1[CH2:9][C:8]1([CH3:11])[CH3:10])=[S:6].[CH3:14][NH2:15]>C1COCC1>[CH3:1][C:2]1([CH3:13])[CH2:4][N:3]1[P:5]([N:7]1[CH2:9][C:8]1([CH3:11])[CH3:10])(=[S:6])[NH:15][CH3:14]참가 물질
4
반응 조건
- 온도
- 4 °C
실험 절차
In a similar manner 0.025 moles of P,P-bis(2,2-dimethyl-1-aziridinyl)thiophosphinic bromide in about 170 milliliters of THF, prepared in accordance with Example 1, is saturated with an excess of gaseous methylamine, stirred over night at 4° C., filtered, concentrated on a rotary evaporator at room temperature, and vacuum distilled to provide about 65% yield of P,P-bis(2,2-dimethyl-1-aziridinyl)-N methylthiophosphinic amide.
후처리
- filtrationfiltered
- concentrationconcentrated on a rotary evaporator at room temperature
- distillationvacuum distilled
출처 및 근거
- ORD 기록
- ord-0951276e791a46f08112c8d5d0d2ff55
- 출처 데이터셋
- uspto-grants-1985_10
- 특허 번호
- US04544501
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