참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chloroacetonitrile | HCID 7856 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 1-Heptanamine, N-ethyl- | HCID 48038 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 20225324 | HCID 20225324 | — |
반응 단계
Combine 7.95 g (0.055 moles) ethyl(heptyl)amine, 3.5 ml (0.055 moles) chloroacetonitrile, 5.8 g (0.055 moles) sodium carbonate and 25 ml toluene in a sealed pressure tube. Heat to 125° C. for 18 hrs. Follow the progress of the reaction by thin layer chromatography on silica gel (CH3CN+MeOH+NH4OH, 85+10+5). At the completion of the reaction, filter the reaction mixture and evaporate the solvents to provide the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04544654 |
|---|
| 출처 데이터셋 | uspto-grants-1985_10 |
|---|
| ORD ID | ord-848d384f4a9e4071b0ce402d368bbeaf |
|---|
| 출처 메모 | uspto-grants-1985_10 |
|---|
