참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | Monomethyl azelate | HCID 75009 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Methyl 9-chloro-9-oxononanoate | HCID 544297 | — |
반응 단계
In a separate process, 23.9 g of azelaic monomethylester was dissolved in 30 ml chloroform. Oxalylchloride (15 ml) was added, all at once, and the mixture refluxed 2 hours at 50° C. The mixture was cooled; excess solvent and oxalylchloride were evaporated. After distillation, 25.8 g of CH3OCO(CH2)7COCl was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04544668 |
|---|
| 출처 데이터셋 | uspto-grants-1985_10 |
|---|
| ORD ID | ord-e70b7d36c96148e3b9e913f07b19395b |
|---|
| 출처 메모 | uspto-grants-1985_10 |
|---|
